Beilstein J. Nanotechnol.2016,7, 637–644, doi:10.3762/bjnano.7.56
humidity. We also investigate a similar film on bulk silicon substrate using grazing-incidence small-angle X-ray scattering (GISAXS), in order to determine nanostructural parameters of the film as well as the water-sorption-induceddeformation of the ordered mesopore lattice. The strain of the mesoporous
bending; grazing incidence small-angle X-ray scattering (GISAXS); mesoporous film; sorption-induceddeformation; Introduction
Because the bending of a microcantilever can be measured with extremely high accuracy, sensors utilizing this principle are in focus of recent research. Such sensors are able, for
most likely induced by the sorption-induceddeformation of the mesoporous film. Therefore, we attribute the strong change in the slope of the curves seen in Figure 2 (about 70% RH for adsorption and about 55% RH for desorption) to the transition from film formation on the pore walls to the spontaneous
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Figure 1:
(a) Scheme of an AFM cantilever coated with a porous silica film in the fluid cell with deflection ...